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Jul 23, 2019 | Blogs, Food / Beverage | 0 comments
When it comes to protecting people from harmful pesticide residues in food, standards around the world are anything but consistent. While the European public has a reasonable level of confidence that their food is below the maximum limits for pesticide residues, it’s a different story for consumers in the United States.
The recent annual EU report on pesticide residues in food found that 95.9% of 88,247 samples from 28 EU states were free of pesticide residues, or contained traces that were below the legally permitted maximum levels. Jump across the Atlantic and America is lagging behind! The nation is using a shocking number of pesticides (1 in 10) that contain ingredients either banned or not approved in not only Europe but also in China and Brazil.
Unfortunately, the difference in pesticide use is typical of many countries around the world, where the guidelines continue to vary considerably. But it’s important to remember that our food supply is global and that the US is the largest exporter of food products worldwide. Regardless of where the produce is grown, there are global standards to consider. While regulatory processes catch up, testing remains the most effective way to protect our food supply from hundreds of pesticides used around the world.Screening Food for Pesticides to Meet Global StandardsFood testing laboratories have traditionally relied on gas chromatography coupled with mass spectrometry (GC–MS) for rapid pesticide detection in large numbers of samples. However, the regulated pesticide list is expanding while the highest permitted levels of pesticide residues in food and feed are becoming even more restrictive. For example, the EU legislation sets a general default maximum residue level (MRL) of 0.01 mg/kg when a pesticide is not specifically mentioned.
What this means is that, to be on the safe side, laboratories need tools that allow them to analyze thousands of substances at low concentrations, in a variety of food and feed samples, such as fruit, vegetables, and animal byproducts. This is where liquid chromatography-tandem mass spectrometry (LC-MS/MS) methods serve as an alternative to GC-MS for comprehensive screening.
LC-MS/MS offers food researchers:
Unfortunately, mass spectrometry systems are typically perceived as expensive and complex–but we’re busting the myth! The SCIEX Triple Quad™ 3500 System provides labs with robust and reliable mass spectrometry technology at an affordable price to efficiently and effectively screen for pesticides.
A Robust and Reliable Pesticide Screening MethodTo demonstrate the capabilities of the Triple Quad 3500 System in pesticide screening, our team developed a method that uses simple, generic extraction procedures and MRM mode to screen food samples for hundreds of pesticides in a single injection.
See how we met a detection limit of 2 ng/mL or lower for these pesticides, with good linearity across 4 orders of magnitude. Download the SCIEX Triple Quad 3500 compendium by filling out the form on your right.
The Echo® MS+ system is a novel platform for Acoustic Ejection Mass Spectrometry (AEMS) and combines the speed of acoustic sampling with the selectivity of mass spectrometry. This platform has been designed for high throughput analysis of small and large molecules. The technology combines Acoustic Droplet Ejection (ADE), an Open Port Interface (OPI) and could be coupled with the SCIEX Triple Quad 6500+ system or the ZenoTOF 7600 system.
The Echo® MS+ system comprises of an open-port interface (OPI) and acoustic droplet ejection (ADE) module which could be coupled with a mass spectrometer. The mass spectrometer could either be a SCIEX Triple Quad 6500+ system or the ZenoTOF 7600 system. This non-liquid chromatography based; high-throughput screening platform enables rapid analysis of compounds at speeds of up to 1 sample/second.
The ability to consistently achieve reproducible results on many complex samples across multiple days is critical to a routine clinical laboratory. Laboratories relying on analytical instrumentation require stability and robustness to perform a variety of screening and confirmatory assays with confidence. Liquid chromatography-tandem mass spectrometry (LC-MS/MS) has become the preferred analytical method in the clinical laboratory to reliably perform clinical testing as it provides best-in-class performance and reliability for the most challenging assays. LC-MS/MS offers the required levels of sensitivity and specificity for the detection and quantitation of molecules from complex biological samples, helping laboratories deliver highly accurate data for a variety of clinically relevant analytes across a wide range of assays.
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